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21.
NiTi形状记忆薄膜的显微结构和力学性能 总被引:3,自引:0,他引:3
NiTi形状记忆合金薄膜具有形状记忆效应,极有希望用于制造高技术领域微电子机械系统中的微型激发器。NiTi形状记忆合金薄膜在制备和使用过程中需要高品质(衬)底材。本文利用高分辨电子显微学和高分辨分析电子显微学详细研究了硅底材NiTi形状记忆合金薄膜的NiTi/Si和NiTi/SiO2微结构体系,包括薄膜精细结构和界面反应。也研究了其显微结构和力学性能的关系。特别给出了NiTi形状记忆合金薄膜产生疲劳过程的微观过程的起因,通过高达十万个使用热循环前后样品显微结构变化的比较,发现纳米尺度上的TiNi3新相的形成导致疲劳过程的发生。如何抑制TiNi3新相形成的研究正在进行之中,这将为进一步提高NiTi形状记忆合金的使用寿命指出方向。 相似文献
22.
Cypriano G da Trindade Neto Ana LP Fernandes Ana IB Santos Waldenice A Morais Marcos VM Navarro Tereza NC Dantas Mrcia R Pereira Jos LC Fonseca 《Polymer International》2005,54(4):659-666
Complexation of chitosan in aqueous solutions by low molecular weight electrolytes is one of the simplest methods for the preparation of aqueous chitosan dispersions. In this work, the influence of storage time, sulfate concentration, method of preparation and surfactant content on some properties of the resultant chitosan dispersions (turbidity, viscosity and zeta potential) was analyzed. Turbidimetry was adequate to monitor the formation of particles, while viscometry was suitable to monitor changes in the dispersing phase. An analysis of the properties of these systems, mainly in terms of particle–particle and macromolecule–macromolecule interactions was carried out. Copyright © 2004 Society of Chemical Industry 相似文献
23.
Aimin Xiang Zhongjie Du Qinghua Zeng Chen Zhang Hangquan Li 《Polymer International》2005,54(10):1366-1370
This paper presents recent efforts on the preparation of flexible polyhedral particles via concentrated emulsion templating polymerization in which the hydrophilic monomer (acrylamide) and hydrophobic monomer (butyl acrylate) are polymerized simultaneously in the continuous and dispersed phase, respectively. Such templating polymerization has been enhanced in our systems owing to the introduction of acrylamide monomer and their higher polymerization rate in continuous phase as compared with butyl acrylate in dispersed phase. Diffusion between the different phases was also inhibited. Furthermore, the stability of the concentrated emulsion and the molecular weight of the produced poly(butyl acrylate) were found to be significantly affected by the amount of redox initiator. The morphology of the particles could be controlled by varying the volume fraction of the dispersed phase and the polyhedral particles were achieved at higher volume fraction. Copyright © 2005 Society of Chemical Industry 相似文献
24.
用化学还原法合成了FeBP非晶态合金超细微粒,用电感耦合等离子体光谱(ICP)、X射线粉末衍射(XRD)、透射电子显微镜(TEM)和差热分析(DSC)等手段对其进行了物性表征,并用微型催化反应装置考察了其对PH3分解的催化作用,结果表明,非晶态合金FeBP对PH3的分解具有良好的催化作用,能使PH3的分解温度从800℃以上降到500℃左右。490℃时分解率超过90%,540℃时达100%。 相似文献
25.
Bedich ika Helena Bendov Ivan Macha
《Chemical Engineering and Processing: Process Intensification》2005,44(12):1312-1319
A procedure has been proposed for the estimation of the terminal falling velocity of non-spherical particles moving in a Carreau model fluid in the transition flow region. The procedure is based on a modification of the relationship formerly developed for the fall of spherical particles including the particle dynamic shape factor. The suitability of the proposed procedure has been confirmed by good agreement between experimental and calculated terminal falling velocity data. In the experiments, the terminal falling velocity of short cylinders and rectangular prisms in polymer solutions of different measure of shear thinning and elasticity has been measured. 相似文献
26.
A method to produce monodisperse magnetic composite spheres with diameters from less than 100 nm to more than 1 μm in water solution is reported. The spheres consist of a dielectric silica core and a cobalt/cobalt oxide shell which can be protected from further oxidation with an outer shell of silica or, alternatively, they can be covered with the polymer polyvinylpyrrolidone as a stabilizer. The formation of a uniform magnetic shell proceeds with the adsorption of metallic cobalt seeds, produced by the reduction of cobalt chloride with sodium borohydride, on a self‐assembled layer of polyelectrolytes on the silica core. In the second step, an outer silica shell can be formed by the hydrolysis and condensation of (3‐aminopropyl)trimethoxysilane and tetraethoxysilane. The double‐shell composite spheres show excellent sphericity, monodispersity, and a magnetic hysteresis loop at room temperature. 相似文献
27.
The iterative finite element model, in which an element is used to represent a single particle, is generated to analyze the
global behavior of multiple-material aggregates of materially nonlinear viscoplastic particles. The generalized Maxwell model
is used to define four types of specific nonlinear viscoplastic materials, which are the elasto visco-plastic matter with
linear viscosity, the plasto visco-plastic material with linear viscosity, the elasto visco-plastic media with nonlinear viscosity,
and the plasto visco-plastic media with nonlinear viscosity. The theory and relevant penalty iterative algorithm are developed
to analyze the four representative mixed granular systems consisting of materially nonlinear viscous particles. To verify
precision of stress calculation, solutions of an axis-symmetric radial flow problem are compared with results of the literature
and they are in a great agreement. The results present here provide significant insight into the fundamental behavior of granular
media under compaction conditions, including prediction of the overall aggregates stress-strain response. 相似文献
28.
Porous NiTi shape memory alloy (SMA) is a novel biomedical material used for human hard tissue implant .The influence of elemental titanium powder characteristics such as powder morphology, particle size and specific surface area( SSA) on the minimal ignition temperature ,combustion temperature and final product of porous Ni-Ti SMA fabricated by combustion synthesis method was investigated in this paper by scanning electron microscopy (SEM) and laser diffraction.The preliminary data indicated that the titanium powder characteristics had a strong effect on combustion synthesis of porous NiTi SMA. 相似文献
29.
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